Diacell® µScopeDAC-HT(S)
Raman and FTIR µSpectroscopy, Pmax = 50 GPa, Tmax = 900 K, WD = 12 mm, A = 51°
Diacell μScopeDAC Series
- The Diacell® μScopeDAC-HT(S) is compatible with commercially available spectroscopic microscopes
- Maximum pressures of up to above 50 GPa are obtained with the Diacell® μScopeDAC-HT(S)
- The DAC is equipped with an internal compact gasket heater that enables research up to 900 K
- A combination of left - and right - handed screws makes sure that there in no net torque on the cell as pressure is applied
- Fitted with type IIas ultra-low fluorescence & ultra-low birefringence diamond anvils the cell is ideal for Infrared and Raman microscopic sample analysis
Description
The Diacell® μScopeDAC-HT(S), manually-driven, high-temperature, diamond anvil cell, meets the growing need to reach very high pressures and be compatible with the optical and physical constraints of microscopes. Temperatures up to above 900 K and pressures up to above 50 GPa are achievable.
The Diacell® μScopeDAC-HT(S) is just 25 mm thick along the optical axis and is symmetrical about the sample. Thus, the physical distance from the objective to the sample between the diamond anvils is just 12 mm. This makes the Diacell® μScopeDAC-HT(S) compatible with most, if not all, commercial Raman and FTIR systems.
Applications
A large and increasing percentage of optical and spectroscopic observations is now made using microscopes. In particular, Raman instruments are commonly sold with integral microscopes to enable efficient scattered light collection, as well as to permit Raman mapping of complex samples. Similarly, FTIR spectrometers are often supplied with reflecting (Cassegrain) microscopes. The Diacell® μScopeDAC-HT(S) is ideal for such applications.
Specifications
| Cell Material | AISI 440C |
| Anvil Support Plate | Tungsten Carbide |
| Pressure Mechanism | Screw driven (RH and LH bolts) |
| Maximum Pressure | 50 GPa |
| Temperature Range | 900 K |
| Top Angle | Conical 51º |
| Bottom Angle | Conical 51º |
| Lateral Access | N/A |
| Heating | Internal gasket heater |
| Cooling | Water cooled |
| DAC Diameter | 60 mm (without any connections) |
| DAC Height | 25 mm |
| Working Distance to Sample | 12 mm |
| Numerical Aperture | 0.44 |
| DAC Weight | 400 g |
Maximum pressure is dependent upon the culet size of the anvils. Almax easyLab is committed to its policy of continuous improvement. Specifications may change without notice. easyLab and Diacell are registered trademarks of Almax easyLab.
Documents
We have compiled a series of technical documents (brochures, articles, technical drawings, …) which you might find useful to help you understand this product better.
Technical documentation
Technical Drawing
Please contact us for further details on the engineering drawings.
Spares, Accessories and Options
Our diamond anvil cells are aligned and mechanically tested before leaving our factory on their way to your laboratory.
They also come supplied with the required basic tooling, including gasket blanks, to use them. All is contained in the transportation casing to move around laboratories easily.
Below you can find some of the accessories and spares you might also consider. If you cannot find what you need, please do not hesitate to contact our team.
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Diamond Anvils 2.5 mm Diacell® design diamond anvils Product code: [P00131] |
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Diamond anvils rings Anvils rings suitable for the μScopeDAC-HT(G) Product code: [M50004], [M50012] |
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Anvil Support Plate Tungsten carbide seat with 52° opening angle Product code: [P00126] |
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Gasket Heater Gasket heater suitable for the μScopeDAC-HT(G) Product code: [A63101] |
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Programmable Power Supply PS-03- Keithley/Temperature Reader including Labview based program Product code: [A75060] |
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Gasket Blanks 10 mm diameter / 0.26 mm thick Inconel gasket blanks Product code: [P02214] |
FAQs
What is the maximum pressure I can achieve with the μScopeDAC-HT(S) and a given culet size?
| Culet size (µm) | 200 | 300 | 400 | 500 | 600 | 800 | 1000 |
| Pmax (GPa) (*) | N/A | 74 | 48 | 31 | 21 | 12 | 8 |
(*) The Pmax values are only indicative. The maximum pressure achievable with a DAC is influenced by many others experimental parameters, like the gasket characteristics (material, thickness and hole size) or the pressure transmitting medium.
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